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Calcium Saccharin USP FCC Food Grade Manufacturers
Anmol Chemicals Group, established in 1976, is the pioneer manufacturer of Specialty Chemicals, Pharmaceutical Excipients, Fragrance & Flavor Chemicals in India. Anmol Chemicals Group has manufacturing facilities spread across Western India, representatives in Houston, Chicago USA and Dubai, UAE. We also have toll manufacturing units for processing chemicals in a few countries around the world. We make IP, BP, USP, NF, Ph. Eur., JP, FCC or Food Grade, Analytical Reagent Grade, LR or Laboratory Reagent Grades and Pure Grades of various chemicals. All our items are analyzed to meet the required standards. We can supply the product in grams for your laboratory trial and in tons for your plant scale jobs.
We manufacture Bulk Drugs / API, Excipients, Pharmaceuticals (IP BP USP NF Ph Eur EP JP), Specialty Chemicals (Pure/Reagent), Mineral Fortifiers (FCC). Our manufacturing facility is FDA approved and GLP, cGMP, ISO9001, ISO14001, ISO/IEC 17025, ISO22000, FSSC 22000, ISO45001, FSSAI, Kosher, HALAL, COPP, WHO-GMP certified and Written Confirmation (WC) is available. Solid materials can be customized for particle size, shape, and bulk density. We observe WHO Good Manufacturing Practices and Good Laboratory Practices. We are a government-recognized STAR Export House and "Authorised Economic Operator (AEO)" per Indian Customs.
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Calcium Saccharin SDS of Manufacturers
CAS Number: 6381-91-5 for Hydrate & 6485-34-3 for Anhydrous, Molecular Weight:467.48, Chemical Formula: C14H8CaN2O6S2-3.5H2O, FEMA: ----,
Calcium Saccharin is used as a sweetner, especially by people restricting their dietary sodium intake. Calcium Saccharin is a sweetener that has been used in food for many years. In cosmetics and personal care products, Calcium Saccharin is used as flavoring agents in the formulation of dental products, mouthwashes and lipstick.
General Specifications of Calcium Saccharin:
Appearance: white crystal or powder
Purity: 98% min.
Melting point: 226C - 230C
Moisture: 15% maximum.
Arsenic: 0.0003% maximum.
Heavy metals: 0.001% maximum.
Arsenous salt: 0.0002% maximum.
Selenium: 0.003% maximum.
Saccharin Calcium USP Grade Specifications:
C14H8CaN2O6S2-3½ H2O - 467.48
C14H8CaN2O6S2 - 404.44
1,2-Benzisothiazol-3(2H)-one, 1,1-dioxide, calcium salt, hydrate (2:7);
1,2-Benzisothiazolin-3-one 1,1-dioxide calcium salt hydrate (2:7) CAS 6381-91-5
Anhydrous CAS 6485-34-3
Saccharin Calcium contains NLT 99.0% and NMT 101.0% of C14H8CaN2O6S2 , calculated on the anhydrous basis.
A. Infrared Absorption
Sample: Dry at 105C to constant weight.
Sample solution: 100 mg/mL
Analysis: To the Sample solution add 2 drops of methyl red, and neutralize with 6 N ammonium hydroxide. Add 3 N hydrochloric acid, dropwise, until the solution is acid to the indicator. Add ammonium oxalat.
Acceptance criteria: A white precipitate is formed when the ammonium oxalate is added. This precipitate is insoluble in 6 N acetic acid but dissolves in hydrochloric acid.
C. Calcium salts moistened with hydrochloric acid impart a transient yellowish-red color to a nonluminous flame.
ASSAYProcedure 1: Limit of Toluenesulfonamides: To pass the test.
Sample solution: 3 mg/mL of Saccharin Calcium in glacial acetic acid. [Note: Slight heating may be needed to dissolve the sample.]
Analysis: Titrate Sample solution with 0.1 N perchloric acid, determining the endpoint potentiometrically. Perform a blank determination, and make any necessary correction. Each mL of 0.1 N perchloric acid is equivalent to 20.22 mg of C14H8CaN2O6S2.
Acceptance criteria: 99.0%–101.0% on the anhydrous basis.
o-Toluenesulfonamide: 10 ppm maximum.
p-Toluenesulfonamide: 10 ppm maximum.
Procedure 2: Limit of Benzoate and Salicylate:
Sample solution: 50 mg/mL
Analysis: To 10 mL of the Sample solution add 5 drops of 6 N acetic acid and 3 drops of ferric chloride.
Acceptance criteria: No precipitate or violet color appears.
Water Determination: NMT 15.0%
Readily Carbonizable Substances:
Sample solution: 40 mg/mL in sulfuric acid (94.5%–95.5% (w/w) of H2SO4), 48C – 50C for 10 min
Acceptance criteria: The Sample solution has no more color than Matching Fluid A, when viewed against a white background.
Clarity of Solution: To pass the test.
Color of Solution: To pass the test.
Packaging and Storage: Preserve in well-closed containers. Store at room temperature.
Calcium Saccharin FCC Food Grade Specifications
1,2-Benzisothiazolin-3-one 1,1-Dioxide Calcium Salt
C14H8CaN2O6S2-31-2H2O Formula weight 467.48
INS: 954 CAS anhydrous 6485-34-3
Calcium Saccharin occurs as white crystals or as a white, crystalline powder. One gram is soluble in 1.5 mL of water.
Function: Nonnutritive sweetener.
A. Dissolve about 100 mg of sample in 5 mL of a 1:20 solution of sodium hydroxide, evaporate to dryness, and gently fuse the residue over a small flame until ammonia no longer evolves. After the residue has cooled, dissolve it in 20 mL of water, neutralize the solution with 2.7 N hydrochloric acid, and filter. Add 1 drop of ferric chloride to the filtrate. A violet color appears.
B. Mix 20 mg of sample with 40 mg of resorcinol, cautiously add 10 drops of sulfuric acid, and heat the mixture in a liquid bath at 200C for 3 min. After cooling, add 10 mL of water and an excess of 1 N sodium hydroxide. A fluorescent green liquid results.
C. A1:10 aqueous solution gives positive tests for Calcium.
D. Add 1 mL of hydrochloric acid to 10 mL of a 1:10 aqueous solution. A crystalline precipitate of saccharin forms. Wash the precipitate well with cold water, and dry at 105C for 2 h. The saccharin thus obtained melts between 226C and 230C.
Assay: Not less than 98.0% and not more than 101.0% of C14H8CaN2O6S2, calculated on the anhydrous basis.
Benzoate and Salicylate: Passes test.
Lead: Not more than 2 mg/kg.
Readily Carbonizable Substances: Passes test.
Selenium: Not more than 0.003%.
Toluenesulfonamides: Not more than 0.0025%.
Water: Not more than 15.0%.
Keywords: Calcium Saccharin IP BP Ph Eur EP USP Analytical Reagent FCC Food Grade Manufacturer Supplier Exporter Monograph Uses Chemical Molecular Formula Weight.
Manufacturer Supplier Exporter
Taloja Mumbai and Ankleshwar, INDIA
Representatives in Houston, Chicago and New York, USA
TEL: (OFF) +91 22 23726950, +91 22 23774610, +91 22 23723564
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Last updated 17-sep-22
Exporters to USA, Canada, UAE, Europe, South Africa, Tanzania, Kenya, Egypt, Turkey, Nigeria, Uganda, Brazil, Chile, Argentina, Dubai, Cameroon, Mexico, Brazil, Chile, Argentina, Korea, Thailand, Malaysia, Indonesia, Australia, China, Germany, France, etc.
Representatives in New York, Houston - Texas, Chicago - Illinois, Los Angeles.
All products are Sold for Industrial Use only. No other use is permitted. Specifications provided are for reference. Grade approvals pending.
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