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for Active Substance to be imported into European Union (EU).Potassium Bromide Commercial Pure & BP Ph Eur USP Analytical Reagent Manufacturers Exporters
Anmol Chemicals is a manufacturer supplier exporter of Potassium Bromide and it offers materials as per IP BP EP Ph Eur USP NF JP FCC Food Grade as per the the latest monograph at best prices. Anmol Chemicals Group, established in 1976, is the pioneer manufacturer of Specialty Chemicals, Pharmaceutical Excipients, Some API, Food Chemicals in India. Anmol Chemicals Group has manufacturing facilities spread across Western India, representatives in Houston, Chicago USA and Dubai, UAE. We also have toll manufacturing units for processing chemicals in a few countries around the world. We make IP, BP, EP, USP, NF, Ph. Eur., JP, FCC or Food Grade, Analytical Reagent Grade, LR or Laboratory Reagent Grades and Pure Grades of various chemicals. All our items are analyzed to meet the required standards. We can supply the product in grams for your laboratory trial and in tons for your plant scale jobs.
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CAS No.: 7758-02-3; EINECS: 231-830-3; Molecular Weight: 119.00; Chemical Formula: KBr
Potassium Bromide SDS of IP BP USP Analytical Reagent FCC Food Grade Manufacturers
Specifications of Commercial Pure Potassium Bromide
Assay: 99.0% KBr
pH of a 5% solution: 4.5.0-9 at 25C
Insoluble matter: 0.05%maximum
Loss on drying: 0.5% maximum
Chloride: 0.5% maximum.
Potassium Bromide BP Ph Eur Grade Specifications
DEFINITION
Content
98.0 per cent to 100.5 per cent (dried substance).CHARACTERS
Appearance
White or almost white, crystalline powder or colourless crystals.
Solubility
Freely soluble in water and in glycerol, slightly soluble in alcohol.IDENTIFICATION
A. It gives reaction of bromides.
B. Solution S (see Tests) gives the reactions of potassium.TESTS
Solution S
Dissolve 10.0 g in carbon dioxide-free water R prepared from distilled water R and dilute to 100 ml with the same solvent.
Appearance of solution
Solution S is clear and colourless.
Acidity or alkalinity
To 10 ml of solution S add 0.1 ml of bromothymol blue solution R1. Not more than 0.5 ml of 0.01 M hydrochloric acid or 0.01 M sodium hydroxide is required to change the colour of the indicator.
Bromates
To 10 ml of solution S add 1 ml of starch solution R, 0.1 ml of a 100 g/l solution of potassium iodide and 0.25 ml of 0.5 M sulphuric acid and allow to stand protected from light for 5 min. No blue or violet colour develops.
Chlorides
Maximum 0.6 per cent.
Iodides
To 5 ml of solution S add 0.15 ml of ferric chloride solution and 2 ml of methylene chloride.
Shake and allow to separate. The lower layer is colourless.
Sulphates
Maximum 100 ppm.
Iron
Maximum 20 ppm.
Magnesium and alkaline-earth metals
Maximum 200 ppm, calculated as Ca.
Heavy metals
Maximum 10 ppm.
Loss on drying
Maximum 1.0 per cent, determined on 1.000 g by drying in an oven at 105C for 3h.
Potassium Bromide USP Grade Specifications
KBr 119.0
Potassium Bromide contains not less than 98.0 percent and not more than 100.5 percent of KBr, calculated on the dried basis. It contains no added substances.
Appearance of solution: clear and colorless.
Test solution— Dissolve 10.0 g in carbon dioxide-free water, and dilute with the same solvent to 100 mL.
Identification—
A: A solution containing 4.5 mg of potassium bromide responds to the test for Bromide.
B: Responds to the test for Potassium.
Acidity or alkalinity— To 10 mL of the solution prepared for the test for Appearance of solution, add 0.1 mL of bromothymol blue TS: not more than 0.5 mL of 0.01 N hydrochloric acid or 0.01 N sodium hydroxide is required to change the color of this solution.
Loss on drying— Dry it at 100 to 105 for 3 hours: it loses not more than 1.0% of its weight.
Bromates—
Starch–mercuric iodide solution— Triturate 1.0 g of soluble starch with 5 mL of water and pour the mixture into 100 mL of boiling water, containing 10 mg of mercuric iodide.
Procedure— To 10 mL of the solution prepared for the test for Appearance of solution add 1 mL of Starch–mercuric iodide solution, 0.1 mL of a 100 g per L solution of potassium iodide, and 0.25 mL of 0.5 M sulfuric acid. Allow to stand protected from light for 5 minutes: no blue or violet color develops.
Limit of chlorine: not more than 0.6%.
Iodides— To 5 mL of the solution prepared for the test for Appearance of solution add 0.15 mL of a 10.5 g per 100 mL ferric chloride solution, and 2 mL of dichloromethane. Shake, and allow to separate. The lower layer is colorless.
Sulfates— A 2.0-g portion shows no more sulfate than corresponds to 0.2 mL of 0.020 N sulfuric acid (0.01%).
Limit of iron: not more than 20 ppm.
Magnesium and alkaline-earth metals— (0.02%, calculated as Ca).
Heavy metals: not more than 10 ppm.
Potassium Bromide Analytical Reagent Grade Specifications
Potassium Bromide
KBr
Formula Weight 119.00
CAS Number 7758-02-3REQUIREMENTS
Assay: 99.0% KBr
pH of a 5% solution: 5.0-8.8 at 25CMAXIMUM ALLOWABLE
Insoluble matter: 0.005%
Bromate (BrO3): 0.001%
Iodate (IO3): 0.001%
Chloride (Cl): 0.2%
Iodide (I): 0.001%
Nitrogen compounds (as N): 0.005%
Sulfate (SO4): 0.005%
Barium (Ba): 0.002%
Heavy metals (as Pb): 5 ppm
Iron (Fe): 5 ppm
Calcium (Ca): 0.002%
Magnesium (Mg): 0.001%
Sodium (Na): 0.02%.Keywords: Potassium Bromide IP BP Ph Eur EP USP Analytical Reagent FCC Food Grade CAS Number 7757-79-1 Manufacturer Supplier Exporter Monograph Uses Chemical Molecular Formula Weight.
Manufacturers
ANMOL CHEMICALS
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Taloja Navi Mumbai, INDIAe-mail: info@anmol.org
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